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USP Proposes Famotidine Monograph Revision Adding Dimaleate Salt Form for Related Compound B

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Summary

USP's Small Molecules Therapeutic Areas 3 Committee proposes revising the Famotidine monograph to introduce the dimaleate salt form of USP Famotidine Related Compound B RS as an alternative to the current hygroscopic free base form. The revision also proposes adopting a two-table format for relative retention times and acceptance criteria, and referencing USP <477> User Determined Reporting Thresholds in the Organic Impurities test. Comments on the proposed Interim Revision Announcement are accepted through November 30, 2026.

“Comments were received indicating that the current free base form of USP Famotidine Related Compound B RS is difficult to handle due to its hygroscopic nature.”

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What changed

The proposed revision modifies the Famotidine monograph's USP Reference Standards <11> section to indicate that USP Famotidine Related Compound B RS may be available as either the free base or the dimaleate salt form, addressing material handling challenges. The monograph structure is also updated to include a two-table format for relative retention times and acceptance criteria, with new references to <477> User Determined Reporting Thresholds in the Organic Impurities test. Additional conforming changes align the monograph with current USP style conventions.\n\nAffected parties—drug manufacturers and quality control laboratories using Famotidine reference standards—should monitor the Pharmacopeial Forum 52(5) publication expected in September-October 2026 and prepare to submit comments by the November 30, 2026 deadline. Firms should review their current reference standard specifications and testing protocols against the proposed changes to assess any necessary updates to analytical procedures or documentation.

Archived snapshot

Apr 28, 2026

GovPing captured this document from the original source. If the source has since changed or been removed, this is the text as it existed at that time.

Notice of Intent to Revise: Famotidine

Type of Posting: Notice of Intent to Revise
Posting Date: 24-Apr-2026
Targeted Official Date: 01-May-2027
Revision Vehicle: Interim Revision Announcement (IRA)
Expert Committee: Small Molecules Therapeutic Areas 3

In accordance with the Rules and Procedures of the Council of Experts, this is to provide notice that the Small Molecules Therapeutic Areas 3 intends to revise the Famotidine monograph.

Comments were received indicating that the current free base form of USP Famotidine Related Compound B RS is difficult to handle due to its hygroscopic nature. To address the comments, it is proposed to introduce the dimaleate salt form of this Reference standard, in addition to its base form, to address improved material handling. Accordingly, the USP Reference Standards <11> section is being revised to indicate that the USP Famotidine Related Compound B RS may be available either as the free base or as the dimaleate salt.

The committee also proposes introducing a two-table format style for relative retention times and acceptance criteria, and adding references to <477> User Determined Reporting Thresholds in the test for Organic Impurities.  Additional changes are also proposed to update the monograph to the current USP style.

It is anticipated that the proposed revision will be published as an Interim Revision Announcement in Pharmacopeial Forum 52(5) [Sep.–Oct. 2026] pursuant to the Rules and Procedures. The comment period for this revision ends on November 30, 2026. In the absence of significant adverse comments, the proposed IRA will become official on May 1, 2027.

Should you have any questions, please contact Ramesh Muppa, Senior Scientist-II (ramesh.muppa@usp.org).

Named provisions

USP Reference Standards <11> Organic Impurities User Determined Reporting Thresholds <477>

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Last updated

Classification

Agency
USP
Published
April 24th, 2026
Comment period closes
November 30th, 2026 (216 days)
Instrument
Consultation
Branch
Independent
Legal weight
Non-binding
Stage
Consultation
Change scope
Minor

Who this affects

Applies to
Pharmaceutical companies Drug manufacturers Healthcare providers
Industry sector
3254 Pharmaceutical Manufacturing
Activity scope
Reference standard specification Monograph revision Drug quality testing
Geographic scope
United States US

Taxonomy

Primary area
Pharmaceuticals
Operational domain
Regulatory Affairs
Compliance frameworks
GxP
Topics
Quality Assurance Intellectual Property

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